Monday, July 11, 2011

What is the best way to use a Vigreux column for fractional-vacuum distillation?

I am trying to distill a water-ethanol mixture using fractional distillation under a vacuum. I am using a stainless steel pot with a very hard, airtight plastic lid. I can cut holes in the lid for the column. What is the best way to set up the column that is vacuum tight?

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